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• W1979596965 abstract "Abstract Pure γ-Gd 2 S 3 was synthesized by the thermolysis of a single Gd[S 2 CN(C 4 H 8 )] 3 phen complex precursor in a flow of argon carrier gas containing sulfur vapor. The complex precursor was decomposed into amorphous Gd 2 S 3 and carbon at about 350 C. Crystalline γ-Gd 2 S 3 could be achieved at temperature exceeding 600 C, and the obtained γ-Gd 2 S 3 presented a very high degree of crystallinity at 800 C. Carbon prevented the formation of Gd 2 O 2 S impurity in the preparation of γ-Gd 2 S 3 . However, the carbon blackened the product. At temperature ≥1000 C, the residual carbon impurity could be efficiently removed by introducing sulfur into the system for the volatile CS 2 could be formed in situ via the reaction of sulfur with the deposited carbon. In the meantime, S also promoted the crystallization of γ-Gd 2 S 3 remarkablely." @default.
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• W1979596965 date "2012-08-01" @default.
• W1979596965 modified "2023-09-27" @default.
• W1979596965 title "Preparation of γ-Gd2S3 via thermolysis of Gd[S2CN(C4H8)]3·phen coordination" @default.
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• W1979596965 doi "https://doi.org/10.1016/s1002-0721(12)60134-3" @default.
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