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- W1979809543 abstract "The Stille reaction of unsymmetric diynes from terminal bromoalkynes with alkynylstannane in the presence of palladium catalyst and cesium fluoride was studied. The system (bromoalkyne: PhC≡CSnMe3:Pd2(dba)3:PPh3:CsF:18-crown-6) = (1:1:0.015:0.06:2.2:0.1) in toluene at reflux temperature was found to be the most favored. Products were obtained in 31–100% yields. Correlations between calculated electron density, dipole moments and 13C NMR spectral data of synthesized bromoacetylenes and diynes have been carried out. Copyright © 2002 John Wiley & Sons, Ltd." @default.
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- W1979809543 date "2002-01-01" @default.
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- W1979809543 title "Synthesis of unsymmetric diynes by palladium and cesium fluoride catalyzed coupling of terminal bromoalkynes with alkynylstannane" @default.
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- W1979809543 doi "https://doi.org/10.1002/aoc.270" @default.
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