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• W1980174830 startingPage "356" @default.
• W1980174830 abstract "The synthesis of 5-(6-mercaptohexyloxy)-1,3-dihydroxybenzene and the formation of a self-assembled monolayer on polycrystalline gold using this compound are described. Methyltrichlorosilane and (tridecafluoro-1,1,2,2-tetrahydrooctyl)trichlorosilane were attached to the 3,5-dihydroxyphenyl terminus of the monolayer. The modified surfaces were studied by contact angle measurement, XPS, and cyclic voltammetry. High contact angles of 119 degrees -128 degrees were observed for the semifluoroalkylsilyl-functionalized monolayer. These high contact angles were maintained after subjecting the surface to, e.g., boiling in water or heating in air to 300 degrees C. Characterization of the silane-modified monolayers by XPS indicated more than one layer of silane present at the top of the monolayer. The thickness was reduced after boiling the cross-linked monolayers in H(2)O, however, maintaining high contact angles. Cyclic voltammetry studies revealed that the semifluoroalkylsilyl-functionalized surface showed a higher blocking capability and a higher electrochemical stability than the parent monolayer." @default.
• W1980174830 created "2016-06-24" @default.
• W1980174830 creator A5064858923 @default.
• W1980174830 creator A5090021722 @default.
• W1980174830 date "2002-11-01" @default.
• W1980174830 modified "2023-09-25" @default.
• W1980174830 title "Attachment of Alkyltrichlorosilanes to the Terminal 3,5-Dihydroxyphenyl Moiety of a Self-assembled Thiol Monolayer on Gold" @default.
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• W1980174830 doi "https://doi.org/10.1006/jcis.2002.8672" @default.
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