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• W1980195590 endingPage "4741" @default.
• W1980195590 startingPage "4735" @default.
• W1980195590 abstract "The step-growth, click polymerization of complementary azide and alkyne-containing monomers to produce polytriazoles (PTAs) has become a versatile and popular method of preparing structurally diverse high molecular weight polymers with a variety of useful functions. We describe here a new class of PTAs that contain 5-iodotriazole linkages prepared by the iodoalkyne version of the copper-catalyzed azide–alkyne cycloaddition (iCuAAC) of an α-azido-ω-iodoalkyne (A–B) monomer. We found this monomer to be highly reactive in the iCuAAC polymerization and show that the resulting poly(5-iodo-1,2,3-triazole) (iodo-PTA) can serve as a useful building block for further postpolymerization derivatization using palladium-catalyzed cross-couplings such as Suzuki and Heck reactions. The parent iodo-PTA and functionalized materials were successfully characterized by various spectroscopic techniques and shown to exhibit a wide range of chemical and thermal properties that are determined by the nature of functionalization at the 5-position of the triazole ring. This data suggests a certain tunability of PTA properties and offers potential for the development of a multitude of useful triazole-based materials based on this postpolymerization functionalization strategy." @default.
• W1980195590 created "2016-06-24" @default.
• W1980195590 creator A5049997949 @default.
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• W1980195590 date "2011-06-02" @default.
• W1980195590 modified "2023-09-27" @default.
• W1980195590 title "Synthesis and Postpolymerization Functionalization of Poly(5-iodo-1,2,3-triazole)s" @default.
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• W1980195590 doi "https://doi.org/10.1021/ma2005469" @default.
• W1980195590 hasPublicationYear "2011" @default.
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