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- W1980230948 abstract "A method is described for the synthesis and purification of 3 alpha-hydroxy-5 alpha-[1,2-3H]pregnan-20-one. [1,2-3H]progesterone (55 Ci/mmol) was incubated with a homogenate of rat brain tissue. The product was purified by Sephadex chromatography and thin-layer chromatography. The identity and purity of the product were established by successive recrystallizations and high-performance liquid chromatography. A 34% portion of the starting material was converted to 3 alpha-hydroxy-5 alpha-[1,2-3H]pregnan-20-one. The final radiopurity of 3 alpha-hydroxy-5 alpha-pregnan-20-one obtained from four independent preparations was 94% to 99%." @default.
- W1980230948 created "2016-06-24" @default.
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- W1980230948 date "1991-11-01" @default.
- W1980230948 modified "2023-09-25" @default.
- W1980230948 title "Synthesis of a [l,2-3H]-labeled pregnanolone" @default.
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- W1980230948 doi "https://doi.org/10.1016/0039-128x(91)90010-s" @default.
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