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- W1980318334 abstract "Complexes [Ag4(mbi:N,N,S)(dppm)4][BF4]2 (1), [Ag4(mpym:N,S)2(dppm)4][BF4]2 (2) and [Ag2(mnic:O,S)(dppm)2]2 (3) with Ag(I) in varied coordination geometries were obtained from the reactions of AgBF4 and the heterocyclic thiolato ligands 2-mercaptobenzimidazole (H2mbi), 2-mercaptopyrimidine (Hmpym) and 2-mercaptonicotinic acid (H2mnic), respectively, with the participation of bis(diphenylphosphino)methane (dppm). The products have been characterized by elemental analyses, IR, 1H and 31P NMR. X-ray crystallographic analyses showed that the structures and the coordination modes are obviously modulated by the thiolato ligands used. With the diazothiolates mbi2− and mpym−, both 1 and 2 contain two closed [Ag2(dppm)2] units connected by the thiolates. When the carboxyl-substituted thiopyridine (H2mnic) was used in 3, a new coordination mode was observed in which the thiolate mnic2− provided an μ3-S to the core of M4(dppm)4 resulting in a neutral complex in which the four Ag atoms are connected by four dppm ligands head-to-tail." @default.
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- W1980318334 date "2003-11-01" @default.
- W1980318334 modified "2023-10-17" @default.
- W1980318334 title "Modulation of the coordination environment of silver(I) in bis(diphenylphosphino)methane complexes by selection of heterocyclic thiolato ligands" @default.
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- W1980318334 doi "https://doi.org/10.1016/s0020-1693(03)00344-x" @default.
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