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- W1980587905 abstract "An improved total synthesis of (8S,11R,12R)- and (8R,11R,12R)-topsentolide B2 diastereomers has been completed in eight steps with overall yields of 10.2% and 10.4%, respectively. The key steps involve a regioselective asymmetric dihydroxylation, diastereoselective Roush allylation, and ring closing metathesis. The stereochemistry of natural topsentolide B2 has been determined to be (8S,11R,12R) by comparison of the specific rotation." @default.
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- W1980587905 date "2011-11-01" @default.
- W1980587905 modified "2023-10-17" @default.
- W1980587905 title "Total synthesis of (8S,11R,12R)- and (8R,11R,12R)-topsentolide B2 diastereomers and assignment of the absolute configuration" @default.
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- W1980587905 doi "https://doi.org/10.1016/j.tetasy.2011.10.020" @default.
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