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• W1980672796 startingPage "10532" @default.
• W1980672796 abstract "We investigated the phase transition behavior from the hexagonally perforated layer (HPL) to the gyroid (G) phase in supported thin film of a polystyrene-b-polyisoprene (PS-b-PI) diblock copolymer (Mn = 34.0 kg/mol, wtPI = 0.634) by grazing-incidence small-angle X-ray scattering. After annealing at 120 °C, the PS-b-PI thin film spin-coated on silicon wafer exhibited HPL morphology with its lamellae highly oriented parallel to the substrate up to a thickness as much as 1 μm. The interface-induced orientation allowed us to obtain a well-developed diffraction pattern in the absence of external mechanical strain to align the domains. The comparison with the computer-simulated diffraction pattern revealed that the HPL structure has mosaic grains oriented randomly in-plane with ABC stacking and undetectable amount of AB stacking. Upon heating, the HPL phase undergoes a phase transition to the G phase. The phase transition occurred epitaxially converting the HPL layers to the {121} planes of the G structure maintaining the G {121} plane oriented parallel to the substrate. This behavior is in contrast with the HPL to G phase transition found from the shear-oriented HPL samples, in which the G {121} plane is randomly oriented around the G [111] axis." @default.
• W1980672796 created "2016-06-24" @default.
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• W1980672796 date "2005-11-12" @default.
• W1980672796 modified "2023-10-07" @default.
• W1980672796 title "Epitaxial Phase Transition of Polystyrene-<i>b</i>-Polyisoprene from Hexagonally Perforated Layer to Gyroid Phase in Thin Film" @default.
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• W1980672796 doi "https://doi.org/10.1021/ma051137i" @default.
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