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- W1980747575 abstract "Urine samples taken from two psychiatric patients who ingested known amounts of the drug dibenzepine hydrochloride were extracted by a two-phase procedure with ether. A first screening by UV spectrophotometry showed the presence of compound(s) with a dibenzepine structure. The TLC separation of aliquots of extracts revealed four spots: two upper spots, each containing two substances, and two lower spots corresponding to single N-demethylated metabolites. GLC on the acetylated extracts by use of a polar column enabled the qualitative and quantitative (with prochlorperazine as internal standard) determinations of free dibenzepine and its five N-demethylated metabolites. IR and mass spectroscopic analyses of these compounds, isolated by micro-preparative GLC of an aliquot of the acetylated extract, confirmed the specificity of results and gave detailed structural information." @default.
- W1980747575 created "2016-06-24" @default.
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- W1980747575 date "1973-01-01" @default.
- W1980747575 modified "2023-09-25" @default.
- W1980747575 title "Improved Method for Determining Dibenzepine and Its N-Demethylated Metabolites in Human Urine" @default.
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- W1980747575 doi "https://doi.org/10.1002/jps.2600620104" @default.
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