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- W1981011997 abstract "Abstract Nanocrystalline (La 1− x Eu x ) 2 Zr 2 O 7 series solid solutions were prepared by a simple and controllable salt-assisted combustion process. The samples were characterized by XRD, TEM and EDS. The results showed the partial substituted products were single-phase solid solutions. The effect of thermal treatment temperature on the crystal size of nanocrystals and the activation energy of crystal growth during calcinations were studied. And the activation energy of (La 1− x Eu x ) 2 Zr 2 O 7 series with x = 0.05, 0.1, 0.25, 0.5, and 0.75 was 25.4, 27.8, 28.0, 32.4, and 30.6 kJ/mol, respectively. TEM images revealed that the products were composed of well-dispersed cubic-like particles with the range of size at 20–50 nm. EDS results furtherly confirmed that the composition of the obtained compound was in agreement with the stiochiometric formular. The emission spectra of (La 1− x Eu x ) 2 Zr 2 O 7 nanocrystals at 385 nm upon excitation showed that there were some intense and prevailing emission peaks located at 590–650 nm." @default.
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- W1981011997 date "2013-02-01" @default.
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- W1981011997 title "A study of Eu-doped La2Zr2O7 nanocrystals prepared by salt-assistant combustion synthesis" @default.
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- W1981011997 doi "https://doi.org/10.1016/j.jallcom.2012.09.004" @default.
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