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• W1981129079 abstract "We investigated the possibility of the interaction of 5-CH3 of thymidine and its 5′-phosphate backbone (C−H···O−−PO3 interaction) in DNA via the insertion of the atomic probe (a selenium atom) into the exo-5-position of thymidine (5-Se-T). 5-Se-T was synthesized for the first time, via Mn(OAc)3 assisted electrophilic addition of CH3SeSeCH3 to 3′,5′-di-O-benzoyl-2′-deoxyuridine. The 5-Se-T phosphoramidite was subsequently synthesized and incorporated into DNA in over 99% coupling yield. Biophysical and structural investigations of the 5-Se-T DNAs revealed that the Se-modified and nonmodified DNAs are virtually identical. In addition, the crystallographic analysis of a 5-Se-T DNA strongly suggests a hydrogen-bond formation between the 5-CH3 and 5′-phosphate groups (CH3···PO4− interaction)." @default.
• W1981129079 created "2016-06-24" @default.
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• W1981129079 date "2009-05-26" @default.
• W1981129079 modified "2023-10-10" @default.
• W1981129079 title "Synthesis and Crystallographic Analysis of 5-Se-Thymidine DNAs" @default.
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• W1981129079 doi "https://doi.org/10.1021/ol9004867" @default.
• W1981129079 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/19469515" @default.
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