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- W1981269820 abstract "The aqueous solution conformation of the 1:1 complexes of ADP and dADP bound to a lanthanide ion have been determined by examination of the dipolar shifts and induced relaxation at pH 6.4. Apparent inconsistencies in the observed data are interpreted in terms of a gradually changing lanthanide-oxygen bond length from Pr3+ to Yb3+. The conformations of ADP and dADP are very similar showing an extended diphosphate, a 2E ribose conformation and with the adenine base displaying a small syn contribution. Relaxation data obtained from Mn(II) titrations are readily interpreted in terms of bidentate coordin ation to α and β phosphates with the nucleotides retaining the same overall conformation found from the lanthanide study. No evidence to support an intramolecular water-bridged background structure is observed. The interaction with Cu(II) is more complex, coordination is observed not only at the diphosphate but also at two sites on the base, N-1. and the chelate formed between N-7 and the amino group. The relative importance of these sites is different for ADP and dADP and is also pH-dependent for ADP." @default.
- W1981269820 created "2016-06-24" @default.
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- W1981269820 date "1979-02-01" @default.
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- W1981269820 title "Determination of the Interaction of ADP and dADP with Copper(II), Manganese(II) and Lanthanide(III) Ions by Nuclear-Magnetic-Resonance Spectroscopy" @default.
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- W1981269820 doi "https://doi.org/10.1111/j.1432-1033.1979.tb12852.x" @default.
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