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- W1981277963 abstract "The metal complexes [Ni{N(Ar)C(R)C(H)Ph}2) (2) (Ar = 2,6-Me2C6H3, R = SiMe3), [Ti(Cp2){N(R)C(But)C(H)R}] (3), M{N(R)C(But)C(H)R}I [M = Ni (4 a) or Pd (4 b)] and [M{N(R)C(But)C(H)R}I(PPh3)] [M = Ni (5 a) or Pd (5 b)] have been prepared from a suitable metal halide and lithium precursor of (2) or (3) or, alternatively from [M(LL)2] (M = Ni, LL = cod; M = Pd, LL = dba) and the ketimine RN = C(But)CH(I)R (1). All compounds, except 4 were fully characterised, including the provision of X-ray crystallographic data for complex 5 a. 1-Azaallyl-Komplexe von NiII, PdII und TiIII Die Metall-Komplexe [Ni{N(Ar)C(R)C(H)Ph}2] (2) (Ar = 2,6-Me2C6H3, R = SiMe3), [Ti(Cp2){N(R)C(But)C(H)R}] (3), M{N(R)C(But)C(H)R}I [M = Ni (4 a) oder Pd (4 b)] und [M{N(R)C(But)C(H)R}-I(PPh3)] [M = Ni (5 a) oder Pd (5 b)] wurden durch Reaktion von Metallhalogeniden mit Lithium-Precursoren von (2) oder (3), beziehungsweise aus [M(LL)2] (M = Ni, LL = cod; M = Pd, LL = dba) und dem Ketimin RN = C(But)CH(I)R (1) hergestellt. Mit Ausnahme von 4 wurden alle Verbindungen vollständig charakterisiert, einschließlich der Kristallstrukturanalyse von Komplex 5 a." @default.
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- W1981277963 date "2000-05-01" @default.
- W1981277963 modified "2023-10-10" @default.
- W1981277963 title "1-Azaallyl Complexes of NiII, PdII, and TiIII" @default.
- W1981277963 doi "https://doi.org/10.1002/(sici)1521-3749(200005)626:5<1081::aid-zaac1081>3.0.co;2-c" @default.
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