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• W1981569149 abstract "Abstract Measurements of 1 H, 19 F, and 31 P NMR, differential scanning calorimetry (DSC) and X‐ray powder diffraction were carried out in piperidinium hexafluorophosphate ([C 5 H 10 NH 2 ]PF 6 ). Three solid phases were observed by DSC in the range from 150 K to the melting point of 517 K. The highest‐temperature phase was determined to form a CsCl‐type cubic lattice with a=6.21(3) Å, Z=1, V =240(4) Å 3 , and D x = 1.60(3) Mg m −3 . From the NMR measurements in this phase, both cation and anion were revealed to perform self‐diffusion as well as isotropic rotation. These molecular motions and thermal properties indicate that this phase is an ionic plastic phase." @default.
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• W1981569149 date "1998-04-01" @default.
• W1981569149 modified "2023-10-18" @default.
• W1981569149 title "Ionic plastic phase in piperidinium hexafluorophosphate studied by solid NMR, X‐Ray diffraction, and thermal measurements" @default.
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• W1981569149 doi "https://doi.org/10.1002/bbpc.19981020408" @default.
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