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- W1981569658 abstract "The distribution of divalent iron and nickel over two metal sites of differing coordination geometry in NiFe 2 (PO 4 ) 2 , sarcopside, has been investigated by resonant X-ray and time-of-flight neutron powder diffraction. To assess the reproducibility of the X-ray technique, data have been collected from instruments X7A at Brookhaven National Laboratory and 8.3 at the Synchrotron Radiation Source, Daresbury Laboratory, England, using wavelengths λ X 1 = 1.7437 (3) Å and λ X 2 = 1.7434 (1) Å, respectively, close to the Fe 2+ K edge determined by X-ray absorption near-edge structure. The real part of the anomalous-scattering correction for iron at each energy, f ′(Fe) X 1 = −7.81 (9) and f ′(Fe) X 2 = −10.16 (6), was determined experimentally by diffraction from Fe 3 (PO 4 ) 2 under identical conditions. Occupancies obtained for iron at the M (1) site were found to be M (1) X 1 = 0.366 (6) and M (1) X 2 = 0.376 (3), compared with M (1) N = 0.26 (15) from time-of-flight neutron powder diffraction." @default.
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- W1981569658 date "1995-10-01" @default.
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- W1981569658 title "Determination of the Cation Distribution in NiFe<sub>2</sub>(PO<sub>4</sub>)<sub>2</sub> using Resonant X-ray and Neutron Powder Diffraction" @default.
- W1981569658 doi "https://doi.org/10.1107/s0021889894012628" @default.
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