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- W1981771576 abstract "Abstract Short polypeptides with four pentad repeats, (VPGVG) 4 and (VPAVG) 4 , were synthesised by manual fluorenylmethoxycarbonyl/ tert ‐butyl (Fmoc/ t ‐Bu) solid phase peptide synthesis using a convergent approach. In the next step, the peptides were coupled via their N ‐terminus with activated semi‐telechelic poly(ethylene glycol) O ‐( N ‐Fmoc‐2‐aminoethyl)‐ O ′‐(2‐carboxyethyl)undeca(ethylene glycol) (Fmoc–PEG–COOH) to yield monodisperse Fmoc‐PEG‐peptide diblock copolymer. Both the presence of the terminal hydrophobic Fmoc group and the hydrophilic PEG chain in the copolymers were shown to play a crucial role in their self‐associative behaviour, leading to reversible formation of supramolecular thermoresponsive assemblies. The peptides and their PEG derivatives were characterised by HPLC, NMR and MALDI‐TOF MS. The associative behaviour of the peptides and their PEG derivatives was studied by dynamic light scattering, MAS NMR and phase contrast microscopy. magnified image" @default.
- W1981771576 created "2016-06-24" @default.
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- W1981771576 date "2007-01-05" @default.
- W1981771576 modified "2023-10-13" @default.
- W1981771576 title "Thermoresponsive Self-Assembly of Short Elastin-Like Polypentapeptides and Their Poly(ethylene glycol) Derivatives" @default.
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- W1981771576 doi "https://doi.org/10.1002/mabi.200600196" @default.
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