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• W1981929934 abstract "X-ray absorption fine structure (XAFS) measurements at the Fe and Mn K-edges were undertaken to investigate the Fe2+-O and Mn2+-O bonding, and Fe2+- and Mn2+-vibrational properties for a series of synthetic almandine-spessartine, (Fe,Mn)(3)Al2Si3O12, garnet solid solutions. The two end members almandine, Fe3Al2Si3O12, and spessartine, Mn3Al2Si3O12, and three solid solutions of composition Alm75Sps25, Alm50Sps50 and Alm25Sps75 were studied at different temperatures between 77 K and 423 K. The spectra show that the state of alternating bonds provides an appropriate description for the two crystallographic ally independent X-O(1) and X-O(2) bonds in the solid solution. An exchange of X-site cations in garnet is associated with measurable structural relaxation. The compositional and temperature dependence of the XAFS Debye-Waller factors for Fe2+ and Mn2+ in the plane of the X-O(1) and the X-O(2) bonds were also determined. Their values in the plane of the X-O(2) bonds are greater compared to those for X-O(1) and they do not vary greatly as a function of garnet composition. In the case of end-member spessartine, the XAFS Debye-Waller factors for Mn2+ are compared to the Debye-Waller factors measured from single-crystal X-ray diffraction. An analysis shows correlation in the atomic displacements along the shorter Mn-O(1) bond." @default.
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• W1981929934 date "2004-10-18" @default.
• W1981929934 modified "2023-09-24" @default.
• W1981929934 title "Fe<SUP>2+</SUP>-O and Mn<SUP>2+</SUP>-O bonding and Fe<SUP>2+</SUP>- and Mn<SUP>2+</SUP>-vibrational properties in synthetic almandine-spessartine solid solutions: an X-ray absorption fine structure study" @default.
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• W1981929934 doi "https://doi.org/10.1127/0935-1221/2004/0016-0801" @default.
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