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• W1981996546 abstract "The first size-selective synthesis of [9]–[11] and [13]cycloparaphenylenes (CPP) has been achieved by strategically utilizing cis-1,4-diphenylcyclohexane-1,4-diyl as the key terphenyl-convertible L-shaped unit. To access the designed triangular or rectangular macrocyclic precursors, we utilized palladium-catalysed C–B/C–Br cross-coupling (Suzuki–Miyaura coupling) and/or nickel-mediated C–Br/C–Br coupling. We also established step-economical routes to [14] and [16]CPP using nickel-mediated C–Br/C–Br coupling. The final aromatization steps toward CPPs were accomplished with NaHSO4. Thus, combined with our previous size-selective synthesis of [12] and [14]–[16]CPP, we completed our size-selective synthesis of [9]–[16]CPP. The successful size-selective syntheses of [n]CPPs speak well for the flexibility and reliability of our strategy using a cyclohexane ring." @default.
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• W1981996546 date "2012-01-01" @default.
• W1981996546 modified "2023-10-13" @default.
• W1981996546 title "Size-selective synthesis of [9]–[11] and [13]cycloparaphenylenes" @default.
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• W1981996546 doi "https://doi.org/10.1039/c2sc20343j" @default.
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