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• W1982034893 startingPage "131" @default.
• W1982034893 abstract "Calcium phosphate (CaP) coatings on Ti6Al4V substrate were elaborated by electrodeposition at different current densities (2, 5 and 10 mA/cm2). The surface morphology and the chemical composition of the coatings were characterized by scanning electron microscopy associated to X-ray microanalysis (SEM-EDXS). However, these CaP coatings are irregular specimens (rough surface, porosity, variable thickness), so the SEM-EDXS analysis becomes limited. Therefore, we carried out an experimental procedure to minimize these effects which is based on global analysis by SEM-EDXS confirmed by a nanometer scale analysis using scanning transmission electron microscopy associated to X-ray microanalysis. Moreover, phase analysis was performed by X-ray diffraction in order to corroborate the chemical characterization and to identify the different calcium phosphate phases as a function of current density. The results showed that at 2 mA/cm2 current density, the coating is composed of an octacalcium phosphate: Ca8H2(PO4)6 and its amorphous phase called OCPam. At 5 mA/cm2, the coating is a mix of calcium deficient hydroxyapatite (Ca-def HAP): Ca10 − x(HPO4)x(PO4)6 − x(OH)2 − x with 0 < × ≤ 2 and its amorphous phase called Ca-def HAPam. And, at 10 mA/cm2, the coating is mainly composed of an amorphous phase of Ca-def HAPam. Furthermore, cathodic reaction mechanisms of electrolytic CaP coatings on Ti6Al4V are proposed to explain the different kinds of calcium phosphate obtained." @default.
• W1982034893 created "2016-06-24" @default.
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• W1982034893 date "2005-12-01" @default.
• W1982034893 modified "2023-10-16" @default.
• W1982034893 title "Characterization of electrodeposited calcium phosphate coatings by complementary scanning electron microscopy and scanning-transmission electron microscopy associated to X-ray microanalysis" @default.
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• W1982034893 doi "https://doi.org/10.1016/j.tsf.2005.07.209" @default.
• W1982034893 hasPublicationYear "2005" @default.
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