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• W1982165789 abstract "Nickel electrodeposits prepared in NiSO4 and NiCl2 electrolytes with thicknesses of 43–49.4 μm were examined by the impedance spectroscopy (IS) method for a–c frequencies 1 Hz–100 kHz. The Nyquist diagrams were single, almost perfect semicircles, suggesting the applicability of the in parallel combination of the Ra–Ca elements characterised by a single relaxation time, 8.27×10−6 s, combined in series with another Rb element, Rb≪Ra. This relaxation time predicted that the incorporated hydrogen atoms are involved in the process of conduction by a hopping/diffusion mechanism, which is differentiated in the cases of NiSO4–Ni and NiCl2–Ni deposits. The diffusion coefficient of hydrogen, 1.25×10−11 cm2 s−1, was determined. The microstructure of Ni electrodeposits was also studied and characterised by electron microscopy. Finally, a general model for the microstructure of Ni electrodeposits, consistent with the results of impedance spectroscopy, was formulated." @default.
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• W1982165789 date "2002-03-01" @default.
• W1982165789 modified "2023-10-16" @default.
• W1982165789 title "Impedance spectroscopy study of nickel electrodeposits" @default.
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• W1982165789 doi "https://doi.org/10.1016/s0167-577x(01)00459-1" @default.
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