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- W1982206056 abstract "Cd2P2S6 crystallizes in a layered structure which is readily intercalated with a variety of Lewis bases. We have studied the intercalation reactions of this lattice with pyridine complexes of several transition metal ions and Ce4+. In some instances (e.g. Mn2+) the metal ion could be co-intercalated with pyridine with little or no effect on the distribution of reaction products formed within the van der Waals gap. However, certain transition metal ions had a dramatic effect on the product distribution obtained. Co-intercalation of Fe3+, for example, results in the production of a highly colored polysulfide species within the van der Waals gap. The intercalated species were identified by mass spectroscopic analysis during thermal de-intercalation. The co-intercalated paramagnetic transition metal ions are useful as ESR spin-probes for the study of the structure and dynamics of the intercalate layer. Analysis of the ESR spectra indicate that co-intercalated Mn2+ can enter Cd2+ lattice vacancies at elevated temperatures." @default.
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- W1982206056 date "1987-01-01" @default.
- W1982206056 modified "2023-10-16" @default.
- W1982206056 title "Spectroscopic and ESR studies of Cd2P2S6 intercalated with pyridine complexes of ferric ion" @default.
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- W1982206056 doi "https://doi.org/10.1016/0022-3697(87)90137-5" @default.
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