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- W1982485514 abstract "Sodium metal mirror reduction of biphenylene in aprotic THF solution containing [2.2.1]cryptand yields as a structurally characterized product the 9,9-dimethylsilafluorene radical anion salt containing a (H3C)2Si expanded cyclobutadiene ring. In addition, the Si content can be detected by total reflection X-ray (TXRF) analysis. When the use of any silicon grease was avoided for all glass fittings, the solvent-separated biphenylene radical anion contact pair crystallized from an aprotic diglyme solution." @default.
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- W1982485514 date "1999-05-15" @default.
- W1982485514 modified "2023-10-14" @default.
- W1982485514 title "Biphenylene Ring Expansion by a (H<sub>3</sub>C)<sub>2</sub>Si Link from Silicone Grease As Proven by the Crystal Structures of [(Sodium<sup>+</sup>[2.2.1]cryptand)(9,9-dimethylsilafluorene<sup>•-</sup>)] as Well as [Sodium<sup>+</sup>(triglyme)<sub>2</sub>(biphenylene<sup>•-</sup>)] and by Total-Reflection X-ray Fluorescence Spectrometry (TXRF)<sup>1</sup>" @default.
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- W1982485514 doi "https://doi.org/10.1021/om9807304" @default.
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