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• W1982539837 abstract "The present work focuses on the partial oxidation of methyl ethyl ketone to acetic acid over TiO2 supported vanadia catalysts with V loadings from 1 to 13.5 wt.%. In order to elucidate the relation between catalytic activity and the structure of the catalysts, the catalysts were also characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), temperature programmed reduction with hydrogen (TPR), and temperature programmed desorption of lattice oxygen (TPD-O2). The investigations show that with increasing V loading the MEK conversion increased whereas the turn-over frequency decreased. At lower V loading (1–4 wt.%) the total oxidation to COx was favoured and the selectivities to acetic acid and other oxygenated products were low. The highest selectivities to acetic acid were achieved at V loadings of 4–6 wt.%. Based on literature data and our results, a scheme of the reaction pathways for the partial oxidation of MEK to AcOH and other by-products was developed." @default.
• W1982539837 created "2016-06-24" @default.
• W1982539837 creator A5046915328 @default.
• W1982539837 creator A5055872442 @default.
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• W1982539837 date "2008-02-01" @default.
• W1982539837 modified "2023-09-25" @default.
• W1982539837 title "Characterization of VOx-TiO2 catalysts and their activity in the partial oxidation of methyl ethyl ketone" @default.
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• W1982539837 doi "https://doi.org/10.1016/j.molcata.2007.11.001" @default.
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