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- W1982733683 abstract "The halogenation of the tin(II) alkyl SnR12 (1) [R1 = CH(SiMe3)C9H6N-8] to give R12SnX2 [X = F (2), Cl (3), Br (4), I (5)] was investigated by reacting 1 with SnX2 (X = F, Cl, Br, and I), PbCl2, BCl3, and X2 (X = Br, I), respectively. 1H, 119Sn NMR and X-ray analysis showed that the reactions with SnX2 under a milder experimental condition afforded intermediate compounds, R12Sn→SnX2 [X = Cl (6), Br (7)] and R1SnX [X = Cl (8), Br (9)]. Further heating gave the final products R2SnX2. The X-ray structures of 2−6 and 9 have been determined. The dynamic exchange process between diastereoisomers of R1SnX (X = Cl, Br) has been studied by variable-temperature 1H and 119Sn NMR spectroscopy." @default.
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- W1982733683 date "2003-03-14" @default.
- W1982733683 modified "2023-10-09" @default.
- W1982733683 title "Structural and Mechanistic Studies of Halogenation of a Tin(II) N-Functionalized Alkyl" @default.
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- W1982733683 doi "https://doi.org/10.1021/om020939o" @default.
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