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• W1983133608 abstract "Abstract Hexacoordinated 3d metal perchlorate complexes with quinoxaline 1-oxide(N-QxO) were prepared and characterized by means of spectral and magnetic studies. Several of the new complexes involve exclusively oxygen-bonded unidentate N-QxO ligands and are probably of the types: [Cr(N-QxO)4(OH2)(OClO3)](ClO4)2·5H2O; [Fe(N-QxO)3(OH2)(OClO3)2](ClO4); and [M(N-QxO)4(OH2)2](ClO4)2·xH2O (MFe, Co, c Ni; x = 1 for Co; x = 6 for Fe or Ni). The rest of the new complexes contain some N- and some O-bonded N-QxO groups; likely formulations for these compounds are: [ Mn(ONC 8 H 6 N) n (NC 8 H 6 NO) 5−n (OClO 3 )](ClO 4 )·4H 2 O ; [ Zn(ONC 8 H 6 N) m (NC 8 H 6 NO) 3−n (OH 2 ) 3 ](ClO 4 ) 2 ; [ Cu(ONC 8 H 6 N)(NC 8 H 6 NO)(OH 2 ) 2 (O 2 ClO 2 )](ClO 4 )·H 2 O; and [ NC 8 H 6 NO) y (ONC 8 H 6 N) 3−y (O 3 ClO)Cu(NQxO) 2 Cu(OClO 3 )(NC 8 H 6 N) 3−y (ONC 8 6 N) y ](ClO 4 ) 2 ·4H 2 O . The latter complex is apparently the only binuclear compound of the series, involving two O-bonded bridging N-QxO ligands, as suggested by its subnormal magnetic moment (0.99 μB). The Fe(III) compound also shows a subnormal μeff (2.61 μB), which was attributed to spin-state equilibria, while the rest of the new complexes with paramagnetic metal ions are magnetically normal high-spin compounds." @default.
• W1983133608 created "2016-06-24" @default.
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• W1983133608 date "1977-01-01" @default.
• W1983133608 modified "2023-09-28" @default.
• W1983133608 title "3d Metal perchlorate complexes with quinoxaline 1-oxide[1]" @default.
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• W1983133608 doi "https://doi.org/10.1016/0022-1902(77)80569-1" @default.
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