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- W1983310972 abstract "Capillary gas chromatography was performed with mass spectrometric detection using a novel microplasma ion source for operation in an element-selective mode. The ion source was a 350 kHz radio frequency helium plasma, which was sustained inside the 4 cm end of a 0.32 mm i.d. fused silica capillary column, and located inside the high vacuum chamber of the quadrupole mass spectrometer. Due to the low volume of the ion source, a stable low pressure discharge was produced utilizing only the 2.25 mL min−1 of GC carrier gas (helium) for plasma support. Small amounts of oxygen (0.1–0.2% v/v) were added to the plasma gas in order to prevent carbon deposits and to enhance signal-to-noise ratios. Chlorine and bromine were selectively detected at the 5–20 pg s−1 level (S/N = 2), and both produced a response that was linear within 3 orders of magnitude." @default.
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- W1983310972 date "1998-05-01" @default.
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- W1983310972 title "Capillary Gas Chromatography Coupled with Microplasma Mass Spectrometry - Improved Ion Source Design Compatible with Bench-Top Mass Spectrometric Instrumentation" @default.
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- W1983310972 doi "https://doi.org/10.1002/(sici)1521-4168(19980501)21:5<282::aid-jhrc282>3.0.co;2-j" @default.
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