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- W1983375560 abstract "Sodium layered oxides with mixed transition metals have received significant attention as positive electrode candidates for sodium-ion batteries because of their high reversible capacity. The phase transformations of layered compounds during electrochemical reactions are a pivotal feature for understanding the relationship between layered structures and electrochemical properties. A combination of in situ diffraction and ex situ X-ray absorption spectroscopy reveals the phase transition mechanism for the ternary transition metal system (Fe–Mn–Co) with P2 stacking. In situ synchrotron X-ray diffraction using a capillary-based microbattery cell shows a structural change from P2 to O2 in P2–Na0.7Fe0.4Mn0.4Co0.2O2 at the voltage plateau above 4.1 V on desodiation. The P2 structure is restored upon subsequent sodiation. The lattice parameter c in the O2 structure decreases significantly, resulting in a volumetric contraction of the lattice toward a fully charged state. Observations on the redox behavior of each transition metal in P2–Na0.7Fe0.4Mn0.4Co0.2O2 using X-ray absorption spectroscopy indicate that all transition metals are involved in the reduction/oxidation process." @default.
- W1983375560 created "2016-06-24" @default.
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- W1983375560 date "2015-04-15" @default.
- W1983375560 modified "2023-09-29" @default.
- W1983375560 title "In Situ X-Ray Diffraction Studies on Structural Changes of a P2 Layered Material during Electrochemical Desodiation/Sodiation" @default.
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- W1983375560 doi "https://doi.org/10.1002/adfm.201500469" @default.
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