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- W1983392007 abstract "Abstract Two rhenium compounds, α-Re2Cl4(dppe)2 and trans-ReCl2(dppe)2, were isolated during the study of the reactivity of Re2Cl6-(P(n-Bu)3)2 with the bidentate phosphine 1,2-bis(diphenylphosphino)ethane (dppe) in the presence of acetonitrile, and a high yield synthetic route was developed for α-Re2Cl4(dppe)2. The structures of α-Re2Cl4(dppe)2 · (C6H6)4, α-Re2Cl4(dppe)2 · (dppe), and trans-ReCl2(dppe)2 · ((CH3)2CO)2 were determined by X-ray crystallography and the following data obtained: α-Re2Cl2(dppe)2 · (C6H6)4, monoclinic P21/c, with a = 14.841(3), b = 12.161(4), c = 18.628(7) A , β = 95.33(3)°, V = 33348(2) A 3 , Z = 2, R1 = 0.0418 , and wR2 = 0.1046; α-Re2Cl4(dppe)2 · (dppe), monoclinic P21/c, with a = 10.695(3), b = 16.858(7), c = 19.710(7) A , β = 101.78(1)° , V = 3479(2) A 3 , Z = 2, R1 = 0.0450 and wR2 = 0.1023; trans-ReCl2(dppe)2 · ((CH3)2CO)2, monoclonic P21./c, with a = 11.507(3), b - 13.519(3), c = 17.243(4) A , β = 96.08(2)°, V = 2667.3(11) A 3 , Z = 2, R1 = 0.0369, wR2 = 0.0887 . Additional characterizations of α-Re2Cl4(dppe)2 were performed with 31P NMR and UV-Vis spectroscopy." @default.
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- W1983392007 date "1998-02-01" @default.
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- W1983392007 title "The synthesis and characterization of trans-ReCl2(dppe)2 and α-Re2Cl4(dppe)2" @default.
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- W1983392007 doi "https://doi.org/10.1016/s0020-1693(97)05726-5" @default.
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