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- W1983711200 abstract "The reaction between copper(I) iodide dissolved in excess NaI and quinaldic acid (H-Quild) afforded two compounds: tris-(2-carboxy quinoline)triiodocopper(I) monohydrate (1) and [(H-Quild)2H]+I−·2H2O (2). Both compounds are characterised by elemental analysis, electronic, IR and Raman spectra. They exhibit charge transfer transitions in the visible region. The crystal structure of complex 1 shows that it consists of the polymeric [Cu2I3]− anion, three H-Quild molecules in zwitterionic form (two of them are linked by a hydrogen bond between the two carboxy groups) and a lattice water molecule. The infinite anionic chain [Cu2I3]− is composed of a fusion of three kinds of rings: rhombus-likeCu2I2, folded Cu2I2, and Cu4I4 in a twisted-chair conformation, in which the Cu(1) atom is tetrahedral whereas the Cu(2) atom is trigonal planar. The thermal decomposition of complex 1 is investigated in nitrogen atmosphere." @default.
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- W1983711200 date "2001-09-01" @default.
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- W1983711200 title "A copper(I) complex containing a new structure of the [Cu2I3]− anion. Reaction of CuI with quinaldic acid and the crystal structure of tris-(2-carboxyquinoline)triiododicopper(I) monohydrate" @default.
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- W1983711200 doi "https://doi.org/10.1016/s0277-5387(01)00776-8" @default.
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