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• W1983800650 abstract "Reaction of Co(η5:η2-C5Me4CH2CH2CH = CH2)(η2-C2H4) (1) with bis(trimethylsilyl)acetylene gives a substitution product Co(η5:η2-C5Me4CH2CH2CHCH2)(η2-Me3SiC≡CSiMe3) (2) which simultaneously contains both an η2-alkene and an η2-alkyne ligand. With 1 substituted alkynes R1C≡C2 (R1 = R2 = CO2Me, Ph; R1 = CO2Me, R2 Ph; = R1 = SiMe3, R2 = H) react to give cyclohexadiene complexes of the type Co(η5:η4-C5Me4CH2CH2C6H3R4) (4, 5, 8, 9). This [2+2+2] cycloaddition involves two molecules of an alkyne and the intramolecularly coordinated CC bond leading to an η4-bonded cyclohexadiene ligand which is linked to the five-membered ring by a CH2CH2 bridge. In the case of diphenylacetylene the cyclobutadiene complex Co(η5-C5Me4CH2CH2CHCH2(η4-C4Ph4) (6) is formed as a byproduct." @default.
• W1983800650 created "2016-06-24" @default.
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• W1983800650 date "1992-03-01" @default.
• W1983800650 modified "2023-09-26" @default.
• W1983800650 title "Functionalized Cyclopentadienyl Ligands, VII ^[1] Cobalt‐Mediated Cyclohexadiene Formation Involving an Intramolecularly Coordinated CC Bond" @default.
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• W1983800650 doi "https://doi.org/10.1002/cber.19921250315" @default.
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