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- W1983854101 abstract "Abstract A novel catalyst, Keggin-type Cs salt of Fe substituted mono lacunary phosphotungstate supported MCM-41 was synthesized from H 3 PW 12 O 40 , FeCl 2 and Cs 2 CO 3 and characterized by different techniques like X-ray diffraction, UV–vis diffused reflectance spectroscopy (UV–vis DRS), nitrogen adsorption–desorption, scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), Raman spectra and Fourier-Transform Infrared Spectroscopy (FT-IR). Diffused reflectance spectra and FT-IR studies confirmed the undegraded Keggin structure of the lacunary salt after supporting it on MCM-41. The material showed its amazing catalytic activity toward two different types of reactions. Among various samples prepared, 50 wt% Fe substituted lacunary salt supported MCM-41 showed remarkable catalytic performances. In acid catalyzed bromination of phenol, it showed 95% conversion obtaining p-bromophenol with 99% selectivity and in case of oxidation of trans-stilbene using hydrogen peroxide oxidant, the same catalyst gave 52% conversion with 99% trans-stilbene oxide selectivity." @default.
- W1983854101 created "2016-06-24" @default.
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- W1983854101 date "2012-12-01" @default.
- W1983854101 modified "2023-09-23" @default.
- W1983854101 title "A facile method for synthesis of Keggin-type cesium salt of iron substituted lacunary phosphotungstate supported on MCM-41 and study of its extraordinary catalytic activity" @default.
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- W1983854101 doi "https://doi.org/10.1016/j.cattod.2012.04.067" @default.
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