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• W1983921707 abstract "A study is made on the conditions and methods of preparation of LiNiO2 and their influence on lithium deficiency. A soft chemistry route by hydroxide precipitation and a classical ceramic method were used. In order to compensate the lithium deficiency in LiNiO2, we used a small excess of lithium precursor (never more than 10 mol%). The different samples were characterized by X-ray powder diffraction, followed by a Rietveld refinement. Optimized synthesis conditions lead to Li1−xNi1+xO2 quasistoichiometric materials with a lithium molar deficiency, x, less than 1%, confirmed by Rietveld refinement. Electron spin resonance (ESR) and magnetic measurements are in agreement with these very low x values. A spin-glasslike behavior is observed for the most stoichiometric sample. The susceptibility shows a maximum at 7.5 K on zero-field cooling and is almost constant below 7.5 K on field cooling. No anomaly of the susceptibility is observed at high temperature, indicating a good homogeneity of all samples. A strong influence of x in a narrow composition range (0.004–0.062) on the electrochemical cycling behavior of the corresponding samples is observed." @default.
• W1983921707 created "2016-06-24" @default.
• W1983921707 creator A5052290943 @default.
• W1983921707 date "2001-03-01" @default.
• W1983921707 modified "2023-10-14" @default.
• W1983921707 title "Synthesis, structural characterization and magnetic properties of quasistoichiometric LiNiO2" @default.
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• W1983921707 doi "https://doi.org/10.1016/s0167-2738(01)00706-8" @default.
• W1983921707 hasPublicationYear "2001" @default.
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