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• W1983994056 endingPage "6766" @default.
• W1983994056 startingPage "6763" @default.
• W1983994056 abstract "The title trisaccharide-serine conjugate 1 constituting the linkage region between glycosaminoglycan and protein in proteoglycan, was synthesized via a trisaccharide p-nitrophenyl (PNP) glycoside prepared by stepwise enzymatic transglycosidation to Xyl-PNP with a β-d-galactosidase. In the second transglycosidation step, partial protection of the disaccharide intermediate, Gal-Xyl-PNP, furnished selective galactosylation at the 3′-position. Cleavage of the PNP group after peracetylation, chemical coupling with serine and final deprotection afforded 1. Fluorescence labeled trisaccharide, Gal(β1-3)Gal(β1-4)Xyl(β)-MU (MU: 4-methylumbelliferyl) (2) was also synthesized in a similar way." @default.
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• W1983994056 date "1996-09-01" @default.
• W1983994056 modified "2023-10-16" @default.
• W1983994056 title "Chemoenzymatic synthesis of Gal(β1-3)Gal(β1-4)Xyl(β)-l-Ser and Gal(β1-3)Gal(β1-4)Xyl(β)-MU by the use of β-d-galactosidase" @default.
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• W1983994056 doi "https://doi.org/10.1016/s0040-4039(96)01462-1" @default.
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