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- W1984217078 abstract "NaBi2AuO5 wurde durch Hydrothermalreaktion aus ‘Bi2O5’, Au2O3 · 2H2O und ges. wäßriger NaOH bei Temperaturen von 300 bis 600°C und Sauerstoffdrucken von 3 · 108 bis 6 · 108 Pa erstmals dargestellt. Nach den Ergebnissen der Röntgenstrukturanalyse (P4b2, a = 1 220,02(6); b = 386,68(3) pm; Z = 4; Rw = 0,022) liegen bisphenoidisch verzerrte AuO4-Gruppen vor, die in c-Richtung gestapelt sind. Die Verknüpfung erfolgt über quadratisch pyramidale BiO5-Baueinheiten. In dieser Raumnetzstruktur besetzt Natrium die vorhandenen Lücken. Synthesis and Crystal Structure of NaBi2AuO5 NaBi2AuO5 was obtained by hydrothermal reaction of ‘Bi2O5’, Au2O3 · 2H2O and saturated aqueous NaOH solution at temperatures from 300 to 600°C and oxygen pressure from 3 × 108 to 6 × 108 Pa for the first time. The crystal structure (P4b2; a = 1 220.02(6) pm; b = 386.68(3) pm; Z = 4; Rw = 0.022) consists of bisphenoidic distorted AuO4 groups, which are stacked in c-direction. They are connected by square pyramidal BiO5 units. Sodium is occupying holes within the Au/Bi/O framework thus formed." @default.
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- W1984217078 date "1994-01-01" @default.
- W1984217078 modified "2023-09-27" @default.
- W1984217078 title "Darstellung und Kristallstruktur von NaBi2AuO5" @default.
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- W1984217078 doi "https://doi.org/10.1002/zaac.19946200108" @default.
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