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W1984227963 abstract "Using electron diffraction, trends in the local structural behaviour of the <svg style=vertical-align:-3.39066pt;width:18.8375px; id=M3 height=15.4 version=1.1 viewBox=0 0 18.8375 15.4 width=18.8375 xmlns:xlink=http://www.w3.org/1999/xlink xmlns=http://www.w3.org/2000/svg> <g transform=matrix(.017,-0,0,-.017,.062,11.112)><path id=x4B d=M667 0h-153l-248 291q-28 32 -54 27v-190q0 -65 14.5 -80t77.5 -20v-28h-260v28q58 5 71 20t13 80v392q0 48 -6 66.5t-22 25.5t-59 10v28h258v-28q-59 -5 -73 -20.5t-14 -81.5v-175q29 6 70 45q101 97 167 178q23 27 20 37t-36 14l-23 3v28h240v-28q-57 -5 -86 -18.5
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q2 -89 11 -177z /></g><g transform=matrix(.017,-0,0,-.017,120.833,12.138)><use xlink:href=#x69/></g><g transform=matrix(.017,-0,0,-.017,125.389,12.138)><use xlink:href=#x4F/></g> <g transform=matrix(.012,-0,0,-.012,138.075,16.212)><use xlink:href=#x33/></g> <g transform=matrix(.017,-0,0,-.017,148.188,12.138)><use xlink:href=#x2B/></g><g transform=matrix(.017,-0,0,-.017,161.939,12.138)><use xlink:href=#x1D465/></g> <g transform=matrix(.017,-0,0,-.017,171.438,12.138)><use xlink:href=#x42/></g><g transform=matrix(.017,-0,0,-.017,181.586,12.138)><use xlink:href=#x61/></g><g transform=matrix(.017,-0,0,-.017,189.048,12.138)><use xlink:href=#x54/></g><g transform=matrix(.017,-0,0,-.017,199.281,12.138)><use xlink:href=#x69/></g><g transform=matrix(.017,-0,0,-.017,203.837,12.138)><use xlink:href=#x4F/></g> <g transform=matrix(.012,-0,0,-.012,216.525,16.212)><use xlink:href=#x33/></g> </svg> (NBT-(<svg style=vertical-align:-0.1638pt;width:9.625px; id=M7 height=7.9499998 version=1.1 viewBox=0 0 9.625 7.9499998 width=9.625 xmlns:xlink=http://www.w3.org/1999/xlink xmlns=http://www.w3.org/2000/svg> <g transform=matrix(.017,-0,0,-.017,.062,7.675)><use xlink:href=#x1D465/></g> </svg>)BT) systems are investigated. In KNN, electron diffraction shows a single plane of diffuse intensity perpendicular to [010] across the entire phase diagram, indicating the existence of ferroelectric disorder along this axis. An additional characteristic pattern of diffuse scattering is also observed, involving rods of diffuse intensity running along the <svg style=vertical-align:-5.56917pt;width:50.799999px; id=M8 height=20.674999 version=1.1 viewBox=0 0 50.799999 20.674999 width=50.799999 xmlns:xlink=http://www.w3.org/1999/xlink xmlns=http://www.w3.org/2000/svg> <g transform=matrix(.017,-0,0,-.017,.062,13.688)><path id=x5B d=M290 -163h-170v866h170v-28q-79 -7 -94 -19.5t-15 -72.5v-627q0 -59 14.5 -71.5t94.5 -19.5v-28z /></g><g transform=matrix(.017,-0,0,-.017,5.927,13.688)><use xlink:href=#x31/></g><g transform=matrix(.017,-0,0,-.017,14.086,13.688)><use xlink:href=#x30/></g><g transform=matrix(.017,-0,0,-.017,22.246,13.688)><use xlink:href=#x30/></g><g transform=matrix(.017,-0,0,-.017,30.405,13.688)><path id=x5D d=M226 -163h-170v27q79 7 94 20t15 73v627q0 59 -15 72t-94 20v27h170v-866z /></g> <g transform=matrix(.012,-0,0,-.012,36.275,17.763)><path id=x70 d=M169 380l92 53q26 16 49 16q80 0 128.5 -56t48.5 -133q0 -108 -72.5 -180.5t-176.5 -91.5q-38 1 -69 18v-131q0 -57 13 -70t71 -18v-27h-236v27q49 5 61 17t12 61v452q0 48 -9.5 58.5t-56.5 16.5v24q66 11 145 43v-79zM169 346v-270q37 -39 94 -39q63 0 101.5 50
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q-4 71 -28 134q17 33 42 46q24 -12 42 -46q-24 -63 -28 -134q36 23 56.5 41.5t45.5 49.5q36 2 61 -13q0 -28 -19 -59q-65 -10 -130 -43q65 -33 130 -43q19 -31 19 -59z /></g> </svg> and <svg style=vertical-align:-5.56917pt;width:50.799999px; id=M9 height=20.674999 version=1.1 viewBox=0 0 50.799999 20.674999 width=50.799999 xmlns:xlink=http://www.w3.org/1999/xlink xmlns=http://www.w3.org/2000/svg> <g transform=matrix(.017,-0,0,-.017,.062,13.688)><use xlink:href=#x5B/></g><g transform=matrix(.017,-0,0,-.017,5.927,13.688)><use xlink:href=#x30/></g><g transform=matrix(.017,-0,0,-.017,14.086,13.688)><use xlink:href=#x30/></g><g transform=matrix(.017,-0,0,-.017,22.246,13.688)><use xlink:href=#x31/></g><g transform=matrix(.017,-0,0,-.017,30.405,13.688)><use xlink:href=#x5D/></g> <g transform=matrix(.012,-0,0,-.012,36.275,17.763)><use xlink:href=#x70/></g> <g transform=matrix(.012,-0,0,-.012,43.125,5.525)><use xlink:href=#x2217/></g> </svg> directions of the perovskite substructure and indicative of octahedral tilt disorder about these axes. Similarly, in the NBT-<i >x</i>BT system, rods of diffuse intensity running along the <svg style=vertical-align:-5.56917pt;width:53.112499px; id=M10 height=20.674999 version=1.1 viewBox=0 0 53.112499 20.674999 width=53.112499 xmlns:xlink=http://www.w3.org/1999/xlink xmlns=http://www.w3.org/2000/svg> <g transform=matrix(.017,-0,0,-.017,.062,13.688)><path id=x27E8 d=M360 -163h-62l-192 430v6l192 430h62l-193 -433z /></g><g transform=matrix(.017,-0,0,-.017,7.083,13.688)><use xlink:href=#x31/></g><g transform=matrix(.017,-0,0,-.017,15.242,13.688)><use xlink:href=#x30/></g><g transform=matrix(.017,-0,0,-.017,23.402,13.688)><use xlink:href=#x30/></g><g transform=matrix(.017,-0,0,-.017,31.561,13.688)><path id=x27E9 d=M307 267l-192 -430h-62l193 433l-193 433h62l192 -430v-6z /></g> <g transform=matrix(.012,-0,0,-.012,38.588,17.763)><use xlink:href=#x70/></g> <g transform=matrix(.012,-0,0,-.012,45.438,5.525)><use xlink:href=#x2217/></g> </svg> directions of the perovskite substructure are observed, again indicating octahedral tilt disorder. Ferroelectric-like disorder is also observed in highly BT doped samples, and a continuous change from the “rhombohedral” structure of NBT to the “tetragonal” structure of NBT-12BT is seen from characteristic variation in observed superstructure reflections. A crystal chemical rationalisation of these results is performed, and the implications for structure and properties are discussed." @default.
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W1984227963 date "2013-01-01" @default.
W1984227963 modified "2023-09-23" @default.
W1984227963 title "Structural Disorder in the Key Lead-Free Piezoelectric Materials, and" @default.
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