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- W1984343024 abstract "A new solid-liquid phase-transfer technique has been used to synthesize aryl difluoromethyl ethers and thioethers. Phenols (or thiophenols) and chlorodifluoromethane, dissolved in a cheap aprotic solvent of low polarity, are contacted with solid sodium hydroxide in the presence of a catalytic amount of tris-(3,6-dioxaheptyl)amine. The work-up of the reaction mixtures is very simple. Although yields are similar in both homogenous and heterogeneous procedures using phenols, improved yields are obtained for thiophenols when using phase-transfer conditions." @default.
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- W1984343024 date "1988-11-01" @default.
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- W1984343024 title "Improvement of the synthesis of aryl difluoromethyl ethers and thioethers by using a solid-liquid phase-transfer technique" @default.
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- W1984343024 doi "https://doi.org/10.1016/s0022-1139(00)81548-1" @default.
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