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• W1984382151 abstract "Abstract An enantiomerically enriched sample (84.3% ee) of (aS)-2-methyl-1-[(((o-triisopropylsilyl)oxy)methyl)phenyl]naphthalene was produced via catalytic asymmetric Suzuki–Miyaura cross-coupling using an atropisomeric naphthamide-derived phosphine (A2phos) as the chiral ligand. After one recrystallization, enantiopurity of the biaryl product was improved to 98.9% ee and its absolute configuration was determined by X-ray crystal structural analysis. Through chemical transformations, the (aS)-enantiomers of 1-[(o-hydroxymethyl)phenyl]-2-methylnaphthalene, 1-[(o-chloromethyl)phenyl]-2-methylnaphthalene, and 2-methyl-1-(o-tolyl)naphthalene were obtained. Several other chiral biaryls were synthesized and stereochemically assigned." @default.
• W1984382151 created "2016-06-24" @default.
• W1984382151 creator A5018641849 @default.
• W1984382151 creator A5040747703 @default.
• W1984382151 date "2011-11-01" @default.
• W1984382151 modified "2023-10-03" @default.
• W1984382151 title "Determination of absolute configuration of 2-methyl-1-(o-tolyl)naphthalene and the related axially chiral biaryls" @default.
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• W1984382151 doi "https://doi.org/10.1016/j.tet.2011.09.107" @default.
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