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- W1984395527 abstract "The M(II)-substituted magnetite (M=Ni, Co and Mn) formation in the wet process in a high magnetic field from 0 to 8 T generated by a superconducting magnet has been studied at the iron ion concentration of 1500 mg/l and the Fe(II)/Fe(III) mole ratios (Rf) of 12 and 21. The particle size of the M(II)-substituted magnetite was about 12 nm at Rf=21 and about 7 nm at Rf =12. The Ni(II) content of the Ni(II)-substituted magnetite at Rf=21 was lower than that at Rf=12. In the Ni(II)-substituted magnetite, the lattice parameter increases with an increase in the magnetic field from 0 to 8 T, indicating that high magnetic fields enhance the formation of the Ni(II)-substituted magnetite (solubility enhancement of Ni(II) to magnetite). Also, the lattice parameter of the Co(II)-substituted magnetite decreased with the increasing magnetic field, however, an increase in the lattice parameter was not found in the Mn(II)-substituted magnetite. The presence of large amounts of vacancies was found in the Ni(II)-substituted magnetite formed in high magnetic fields by XRD and atomic absorption analysis. This result is supported by the experimental result in which the magnetite formed in a high magnetic field tends to adsorb Ni(II) in a high magnetic field, and results in the higher incorporation of Ni(II) into the spinel structure." @default.
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- W1984395527 date "2003-01-01" @default.
- W1984395527 modified "2023-09-25" @default.
- W1984395527 title "A high magnetic field effect on the M(II)-substituted magnetite formation (M=Ni, Mn, Co) in the wet process" @default.
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- W1984395527 doi "https://doi.org/10.1016/s0304-8853(02)00582-6" @default.
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