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• W1984487866 startingPage "1843" @default.
• W1984487866 abstract "The LCNn-BuSnCl2 where LCN is 2-(N,N-dimethylaminomethyl)phenyl- as a chelating ligand was reduced by one molar equivalent of potassium to distannane LCNn-Bu(Cl)Sn–Sn(Cl)n-BuLCN (3). The same reduction of LCN2SnCl2 led essentially quantitatively to the stannylene LCN2Sn. Distannane 3 can be oxidized to corresponding organotin(IV) chalcogenides (LCNn-Bu(Cl)Sn-Y-Sn(Cl)n-BuLCN, where Y is O, S, Se, and Te). The structure of these chalcogenides was evaluated by multinuclear NMR spectroscopy techniques and X-ray crystallographic techniques for sulfide, revealing two diastereomeric pairs with the centre of chirality at the tin atoms for all compounds. The further reduction of 1 by excess of reducing agents gave tetranuclear compound [LCN(n-Bu)SnCl]-Sn-{[Sn(n-Bu)LCN]2(μ-Cl)} (10) and LCN(n-Bu)2SnCl. The product of reduction of 3 by K(BEt3)H.THF is the complex 10 as well. The structure and bonding properties in 10 were conducted at DFT theory level." @default.
• W1984487866 created "2016-06-24" @default.
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• W1984487866 date "2010-07-01" @default.
• W1984487866 modified "2023-10-14" @default.
• W1984487866 title "Reduction of C,N-chelated Diorganotin(IV) Dichlorides" @default.
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• W1984487866 doi "https://doi.org/10.1016/j.jorganchem.2010.04.019" @default.
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