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- W1984592314 abstract "The utility of the J-HSMQC experiment to detect long-range CH correlations was investigated. Two new long-range J-compensated pulse sequences, LR-J-HSMQC(80,27) and LR-J-HSMQC(27,80), were developed using the (3βx)βy composite 90° pulse sequence. These two experiments were shown to be effective for long-range coupling constants, nJCH, that were greater than 3 Hz. Although the overall sensitivities of the long-range J-HSMQC experiments were slightly lower than that of the conventional decoupled HMBC experiment, their 2D maps showed additional cross peaks that could be useful in structure elucidation. LR-J-HSMQC(27,80) was very efficient in yielding two- and four-bond relay correlations. The utility of the new sequences is demonstrated with strychnine as the sample." @default.
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- W1984592314 date "2002-06-01" @default.
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- W1984592314 title "Experiments to Detect Long-Range Heteronuclear Shift Correlations: LR-J-HSMQC" @default.
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- W1984592314 doi "https://doi.org/10.1006/jmre.2002.2563" @default.
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