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• W1984663962 endingPage "510" @default.
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• W1984663962 abstract "Pentacoordinated aminosulphur (IV) trifluorides, R2NSF3, (in this paper the lone pair in S(IV)-derivatives is always considered as a ligand) and aminosulphur(VI)-oxidetrifluorides, R2NS(O)F3, readily lose a fluoride ion to Lewis acids (AsF5, SbF5, BF3) to give sulphur-containing cationic species [R2NSF2]+ and [R2NS(O)F2]+ with tetracoordinated sulphur. Tetracoordinated neutral dialkylaminosulphur(IV)-oxidefluorides, R2NS(O)F, and amino-imino sulphur(IV)fluorides, R2NS(=NRf)F, give three-coordinated sulphur cations [R2NSO]+] or [R2NSNRf]+.The three-coordinated sulphur(VI)cation [R2NS(O)NR]+ has also been formed. Die pentakoordinierten Aminoschwefeltrifluoride, R2NSF3 (in dieser Arbeit wird das freie Elektronenpaar in S(VI)verbindungen immer als Ligand betrachtet) und -oxidschwefeltrifluoride, R2NSOF3, geben leicht ein Fluoridion an Fluor-Lewis-Säuren (AsF5, SbF5, BF3) ab unter Bildung der entsprechenden kationischen Spezies [R2NSF2]+ und [R2NSOF2+] mit tetrakoordiniertem Schwefel. Aus den tetrakoordinierten neutralen Dialkylaminosulfinylfluoriden, R2NSOF, bzw. den Amino-Imino-Sulfinylfluoriden, bilden sich durch Fluorid-Ionen-Abstraktion die entsprechenden dreifach koordinierten Kationen [R2NSO]+ bzw. [R2NSNRf]+. Mit dem [R2NS(O)NR]+ gelang die Darstellung eines dreifach koordinierten Kations des S(VI)." @default.
• W1984663962 created "2016-06-24" @default.
• W1984663962 creator A5016877578 @default.
• W1984663962 creator A5045547919 @default.
• W1984663962 date "1979-12-01" @default.
• W1984663962 modified "2023-10-16" @default.
• W1984663962 title "Amino-sulphur-fluorine derivatives as fluoride ion donors: preparation of three- and four-coordinated cations of sulphur (IV) and (VI) [1,2]" @default.
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• W1984663962 doi "https://doi.org/10.1016/s0022-1139(00)82525-7" @default.
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