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• W1984846315 endingPage "1971" @default.
• W1984846315 startingPage "1968" @default.
• W1984846315 abstract "Abstract Azacalixarene 1 , with a relatively long chain substituent, can exhibit both inter‐ and intramolecular CH ··· π interactions. In the crystalline state, the 4‐phenybutyl group is included in the molecular cavity, allowing interactions between the methylene H atoms and the aromatic rings of the azacalix skeleton. In addition, similar “edge‐to‐face” interactions occur between the terminal phenyl ring and that of an adjacent molecule, thus forming a polymeric, supramolecular array of azacalixarene molecules. In solution, the 4‐phenylbutyl arm adopts two orientations, one included in the calix cavity, one not, giving rise to isomers describable as exo and endo conformers. Characterization of the exo / endo equilibrium as a function of temperature by 1 H NMR spectroscopy enabled estimation of the enthalpy difference favoring inclusion attributed to the intracavity CH ··· π interactions." @default.
• W1984846315 created "2016-06-24" @default.
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• W1984846315 date "2011-02-15" @default.
• W1984846315 modified "2023-10-17" @default.
• W1984846315 title "<i>N</i>‐(4‐Phenylbutyl)azacalix[3.1.1.1]arene: Self‐Inclusion of the Side Chain through CH···π Interactions" @default.
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• W1984846315 doi "https://doi.org/10.1002/ejoc.201001460" @default.
• W1984846315 hasPublicationYear "2011" @default.
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