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- W1984973083 abstract "Diphenylphosphorylazide N3P(O)(OPh)2 reacts with Pt(PPh3)3, Pt(PPh3)2(C2H4), trans-RhCl(CO)(PPh3)2, Ru(CO)3(PPh3)2, CoCl2(PPh3)2 and CuCl(PPh3)2 to give the azido complexes Pt(PPh3)2(N3)R, Pt(PPh3)2(N3)2R2, the urylene complex RhCl(PPh3)2(RNCONR) and the phosphine imine complexes Ru(CO)3(RPPh3)2, CoCl2(RNPPh3)2, CuCl(RNPPh3)2, respectively, (RP(O)(OPh)2). The oxidative addition of n-C6F13SO2N3 to Pt(PPh3)4 and Pt(PPh3)2(C2H4) affords the complexes Pt(PPh3)2(N3)R and Pt(PPh3)2(N3)2R2, respectively, (RSO2C6F13. The compounds are characterized by elemental analysis and by their IR spectra.Diphenylphosphorylazid N3P(O)(OPh)2 setzt sich mit Pt(PPh3)3, Pt(PPh3)2(C2H4), trans-RhCl(CO)(PPH3)2, Ru(CO)3(PPh3)2, CoCl2(PPh3)2 bzw. CuCl(PPh3)2 zu den Azidokomplexen Pt(PPh3)2(N3)R, Pt(PPh3)2(N3)2R2, zum Urylenkomplex RhCl(PPh3)2(RNCONR) bzw. zu den Phosphiniminkomplexen Ru(CO)3(RNPPh3)2, CoCl2(RNPPh3)2, CuCl(RNPPh3)2 um (R P(O)(OPh)2). Die oxidative Addition von n-C6F13SO2N3 an Pt(PPh3)4 bzw. Pt(PPh3)2(C2H4) liefert die Verbindungen Pt(PPh3)2(N3)R bzw. Pt(PPh3)2(N32R2 (R SO2-n-C6F13). Die Komplexe werden durch Elementaranalyse und durch ihre IR-Spektren charakterisiert." @default.
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- W1984973083 date "1977-08-01" @default.
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- W1984973083 title "The reactivity of a thermally unstable perfluoroalkylsulfinyl azide" @default.
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- W1984973083 doi "https://doi.org/10.1016/s0022-1139(00)82684-6" @default.
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