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- W1985155083 abstract "The syntheses of methoxy substituted benzocyclobutenone and benzocyclobutenedione tricarbonylchromium complexes rac-4 and rac-10 are reported. rac-4 is preferentially obtained by a [2+2] cycloaddition of 3-methoxy-1,2-dehydrobenzene with diethoxyethene followed by complexation and acetal hydrolysis, whereas rac-10 is prepared by acetalization of the ligand followed by complexation and hydrolysis. rac-4 is stereoselectively reduced to the benzocyclobutenol complex with LiAlH4 in high yield. However, the anion driven ring opening–cycloaddition sequence furnished only poor selectivity. Vinyl Grignard addition to the 3-methoxybenzocyclobutenedione complex rac-10 gave the 1-vinyl adduct, which was characterized by an X-ray structure analysis." @default.
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- W1985155083 date "1999-12-01" @default.
- W1985155083 modified "2023-10-09" @default.
- W1985155083 title "Tricarbonylchromium complexes with methoxy substituted benzocyclobutenone and benzocyclobutenedione ligands" @default.
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- W1985155083 doi "https://doi.org/10.1016/s0020-1693(99)00353-9" @default.
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