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- W1985230270 abstract "A silica-supported molybdenum complex 2 was prepared and found to promote ring-closing alkyne metathesis (RCAM). Thus, the reaction of trisamidomolybdenum(VI) complex 1 with fumed silica in trichlorobenzene gave molybdenum catalyst 2. The RCAM of diyne 3 was carried out under reduced pressure conditions (1 mmHg to remove 3-hexyne) in the presence of 5 mol% Mo of the catalyst 2 to give cyclic product 4 in 62% yield. The RCAM of several diynes gave the corresponding cyclic products in good yield (3 examples: 65-67% yield)." @default.
- W1985230270 created "2016-06-24" @default.
- W1985230270 date "2008-08-22" @default.
- W1985230270 modified "2023-10-17" @default.
- W1985230270 title "Silica-Supported Alkyne Metathesis Catalyst: Synthetic Application" @default.
- W1985230270 doi "https://doi.org/10.1055/s-2008-1078653" @default.
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