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• W1985489247 abstract "FeIIFeIII2F8(H2O)2 and MnFe2F8(H2O)2, grown by hydrothermal synthesis (P ⋍ 200 MPa, T = 450 or 380°C), crystallize in the monoclinic system with cell dimensions (Å): a = 7.609(5), b = 7.514(6), c = 7.453(4), β = 118.21(3)°; and a = 7.589(6), b = 7.503(8), c = 7.449(5), β = 118.06(3)°, and space group C2m, Z = 2. The structure is related to that of WO3 · 13H2O. It is described in terms of perovskite type layers of Fe3+ octahedra separated by Fe2+ or Mn2+ octahedra, or in terms of shifted hexagonal bronze type layers. Both compounds present a weak ferromagnetism below TN (157 and 156 K, respectively). Mössbauer spectroscopy points to an “idle spin” behavior for FeIIFeIII2F8(H2O)2: only Fe3+ spins order at TN, while the Fe2+ spins remain paramagnetic between 157 and 35 K. Below 35 K, the hyperfine magnetic field at the Fe2+ nuclei is very weak: Hhf = 47 kOe at T = 4.2 K. For MnFe2F8(H2O)2, Mn2+ spin disorder is expected at 4.2 K. This “idle spin” behavior is due to magnetic frustration." @default.
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• W1985489247 date "1984-07-01" @default.
• W1985489247 modified "2023-10-17" @default.
• W1985489247 title "Idle spin behavior of the shifted hexagonal tungsten bronze type compounds FeIIFeIII2F8(H2O)2 and MnFe2F8(H2O)2" @default.
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• W1985489247 doi "https://doi.org/10.1016/0022-4596(84)90113-0" @default.
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