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- W1985653473 abstract "The IR spectra of [(CO)4WI]2, Co2(CO)8, Co3(CO)9CCl, Co3(CO)9COMClCp2, (M = Ti, Zr, Hf) and [Co3(CO)9CO]2MCp2 (M = Ti. Zr, Hf) under high pressure have been measured down to 250 cm−1 by using a high pressure cell with diamond or corundum windows. The results obtained have suggested that the symmetries of these polynuclear metal carbonyls, except [Co3(CO)9CO]2TiCp2, are resistant to pressure. On the basis of the pressure dependence of the observed frequencies, the assignments of the observed bands, especially those in the region from 1000 to 250 cm−1, have been made for [(CO)4WI]2, Co2(CO)8 and Co3(CO)9CCl. These assignments have been ascertained with the results of the normal mode calculations. Unter Verwendung einer Hochdruckzelle mit Diamant- bzw. Korundfenstern wurden die IR-Spektren von [(CO)4WI]2, Co2(CO)8, Co3(CO)9CCl, Co3(CO)9COMClCp2 (M = Ti, Zr, Hf) und [Co3(CO)9CO]2MCp2 (M = Ti, Zr, Hf) bei hohen Drücken bis zu 250cm−1 aufgenommen. Diese Metallcarbonyle außer [Co3(CO)9CO]2TiCp2 haben sich als druckresistent bezüglich ihrer Symmetrie erwiesen. Auf Grund der Druckabhängigkeit der beobachteten Frequenzen wurden die beobachteten Banden von [(CO)4WI]2, Co2(CO)8 und Co3(CO)9CCl, insbesondere diejenige im Bereich von 1000 bis 250 cm−1, zugeordnet. Diese Zuordnungen wurden durch Rechenresultate der Normalschwingungen festgestellt." @default.
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- W1985653473 date "1979-10-01" @default.
- W1985653473 modified "2023-09-27" @default.
- W1985653473 title "Infrared Spectra of Polynuclear Metal Carbonyls under High Pressure" @default.
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- W1985653473 doi "https://doi.org/10.1002/bbpc.19790831014" @default.
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