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- W1985830392 abstract "Abstract The two long‐chain dimethylphosphinic amides Me 2 P(X)NH{C 6 H 4 ‐ p ‐[OCO(C 6 H 4 ‐ p ‐OC 8 H 17 )]} (X = S, O) were synthesized by reacting Me 2 PNEt 2 with H 2 N{C 6 H 4 ‐ p ‐[OCO(C 6 H 4 ‐ p ‐OC 8 H 17 )]} and by subsequently achieving the appropriate oxidation step (with H 2 O 2 or S 8 ). The sulfido compound was characterized by X‐ray crystallography, proving to be triclinic, space group, P 1¯, a = 6.056(2), b = 8.110(2), c = 25.016(5) Å, α = 97.04(2), β = 89.91(2), γ = 102.81(3), V = 1188.6(5) Å 3 , Z = 2. In the solid state, the molecule adopts a bent structure with a length of ca . 24 Å." @default.
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- W1985830392 date "2004-07-27" @default.
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- W1985830392 title "Synthesis and Crystal Stucture of a Long-Chain Thiophosphinic Amide, Me2P(S)NH{C6H4-p-[OCO(C6H4-p-OC8H17)]}" @default.
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- W1985830392 doi "https://doi.org/10.1002/zaac.200400027" @default.
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