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- W1985962012 abstract "STRUCTURAL STUDIES OF THE TITLE COMPOUND [SYSTEMATIC NAME: 2,2'-(disulfanedi-yl)dianiline], C(12)H(12)N(2)S(2), were previously performed at room temperature [Gomes de Mesquita (1967 ▶). Acta Cryst.23, 671; Lee & Bryant (1970 ▶). Acta Cryst. B26, 1729; Ribar et al. (1975 ▶). Bull. Yugoslav. Crystallogr. Centre, A10, 68]. The results of the current redetermination allow a clarification of the nature of the intra- and inter-molecular N-H⋯S hydrogen bonding described in the literature for this compound. On cooling to 100 K, the unit cell contracts most in the c axis, and it changes rather less in the directions involving the strongly hydrogen-bonded chains, which are the a and b axes. In the crystal structure, N-H⋯N hydrogen bonds link neighbouring mol-ecules into two-dimensional frameworks parallel to the ab plane. An additional inter-molecular N-H⋯S hydrogen bond has also been established, based on freely refined H-atom positions. Inter-molecular C-H⋯π inter-actions further stabilize the crystal structure." @default.
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- W1985962012 date "2010-01-09" @default.
- W1985962012 modified "2023-10-16" @default.
- W1985962012 title "2,2′-Dithiodianiline: a redetermination at 100 K" @default.
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- W1985962012 doi "https://doi.org/10.1107/s1600536810000024" @default.
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