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- W1986014780 abstract "Oligoethylene (OE) was found to form inclusion complexes with α-cyclodextrin (α-CD) not only from aqueous solutions of α-CD but also from DMF solutions of α-CD to give stoichiometric compounds in a crystalline state in high yields. The yields depend on the oligomeric degree (n) of OE when DMF was used as solvent. OE of n less than 6 did not form complexes with α-CD in DMF solution. The complexes were characterized by IR, 1H NMR, 13C NMR, and 13C CP/MAS and PST/MAS NMR spectra, X-ray (powder), and elemental analysis. The continuous variation plots for the complex formation and the 1H NMR spectra of the complexes show that the stoichiometry of the crystalline complexes is 3 : 1 (ethylene unit–α-CD). The X-ray powder pattern of α-CD–OE complexes and the solid state 13C CP/MAS, PST/MAS NMR spectra suggest that the OE chain is included in the channel formed by α-CD molecules and that the OE backbone in the complexes is more flexible than that in uncomplexed state (OE crystal) due to being included in the cavit..." @default.
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- W1986014780 date "1994-10-01" @default.
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- W1986014780 title "Formation of Inclusion Complexes of Oligoethylene and Its Derivatives with<i>α</i>-Cyclodextrin" @default.
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